Exodus 9:29-35
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29 And Moses said unto him, As soon as I am gone out of the city, I will spread abroad my hands unto the LORD; and the thunder shall cease, neither shall there be any more hail; that thou mayest know how that the earth is the LORD's.
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30 But as for thee and thy servants, I know that ye will not yet fear the LORD God.
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31 And the flax and the barley was smitten: for the barley was in the ear, and the flax was bolled.
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32 But the wheat and the rie were not smitten: for they were not grown up.
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33 And Moses went out of the city from Pharaoh, and spread abroad his hands unto the LORD: and the thunders and hail ceased, and the rain was not poured upon the earth.
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34 And when Pharaoh saw that the rain and the hail and the thunders were ceased, he sinned yet more, and hardened his heart, he and his servants.
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35 And the heart of Pharaoh was hardened, neither would he let the children of Israel go; as the LORD had spoken by Moses.